Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Fluoro-3-nitrobenzotrifluoride → 2,4-Hexadiyn-1,6-diol bis-(2-nitro-4-trifluoromethylphenyl)ether
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Fluoro-3-nitrobenzotrifluoride | HCID 67778 | — |
| 반응물 | Diacetylene glycol | HCID 94973 | — |
| 생성물 | 2,4-Hexadiyn-1,6-diol bis-(2-nitro-4-trifluoromethylphenyl)ether | HCID 88687710 | — |
반응 단계
Reaction of 2,4-hexadiyne-1,6-diol (1 g) with 4-fluoro-3-nitro-benzotrifluoride (4 g.) following the procedure of Example 3 yielded the desired product. Recrystallization from ethanol gave pale yellow needles. (1.1 g., 25%) m.p. 137° C. I.R. (KBr): 1620(NO2), 1120 682 (CF3)cm-1.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04581315 |
| 출처 데이터셋 | uspto-grants-1986_04 |
| ORD ID | ord-3c586a1186c748db81cc0bdcf05a56e3 |
| 출처 메모 | uspto-grants-1986_04 |