HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloranil → HCID 3335773, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloranil | HCID 8371 | — |
| Reactant | Phthalimide potassium salt | HCID 24194345 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 3335773 | HCID 3335773 | — |
Reaction Steps
A suspension of chloranil (10.00 g, 0.04 mole) and potassium phthalimide (30.00 g, 0.16 mole) in acetonitrile is refluxed overnight. The deep purple solution is allowed to cool and then filtered, yielding a tan solid. This solid is then boiled in approximately 200 ml of dimethylformamide for ten minutes. The hot DMF suspension is then filtered yielding a white thixotropic solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04581349 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-4f104052e77947099da9ed2864aa4cf1 |
| Source note | uspto-grants-1986_04 |