HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13580516, compound → HCID 13580515, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13580516 | HCID 13580516 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 13580515 | HCID 13580515 | — |
Reaction Steps
A solution of tetrahydro-3,5-dioxo-1H-pyrrolo[1,2-c]imidazole-2(3H)-acetic acid benzyl ester (2.9 g, 0.01 mol) in tetrahydrofuran, 250 ml, is treated with H2 gas in the presence of a Pd/C catalyst. After H2 uptake is complete, the solution is filtered through filter aid and concentrated in vacuo to yield tetrahydro-3,5-dioxo-1H-pyrrolo[1,2-c]-imidazole-2(3H)-acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04582838 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-15e4659db7f64bd1891c51f020495852 |
| Source note | uspto-grants-1986_04 |