Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Dichloromaleic anhydride | HCID 70728 | — |
| Reactant | (1,3-dimethyl-3-phenylbutyl)amine(SALTDATA: HCl) | HCID 13290299 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 178442356 | HCID 178442356 | 682.7% |
Reaction Steps
16.7 g (0.1 mol) of dichloromaleic anhydride and 17.7 g (0.01 mol) of 3-phenyl-1,3,3-trimethylpropylamine are stirred in 100 ml of glacial acetic acid under reflux for 4 hours. 50 ml of water are added and the mixture is cooled to 20° C. The product is filtered off with suction and dried. 23.5 g (72% of theory) of dichloromaleic acid N-(3-phenyl-1,3,3-trimethylpropyl)-imide of melting point 106°-109° C. are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04582849 |
|---|
| Source dataset | uspto-grants-1986_04 |
|---|
| ORD ID | ord-97502894486c4d1282e18e1f9c9c1fd3 |
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| Source note | uspto-grants-1986_04 |
|---|
