N,N-Diethylethylenediamine → HCID 13590120, compound

HRID 1380616Notes

Reaction equation

HRID 1380616 reaction equation
Cl[C:2]1[C:15]2[C:14](=[O:16])[C:13]3[C:8](=[CH:9][C:10]([O:17][CH3:18])=[CH:11][CH:12]=3)[S:7][C:6]=2[C:5]([N+:19]([O-:21])=[O:20])=[CH:4][CH:3]=1.[CH2:22]([N:24]([CH2:28]C)[CH2:25][CH2:26][NH2:27])C>>[CH3:22][N:24]([CH3:28])[CH2:25][CH2:26][NH:27][C:2]1[C:15]2[C:14](=[O:16])[C:13]3[C:8](=[CH:9][C:10]([O:17][CH3:18])=[CH:11][CH:12]=3)[S:7][C:6]=2[C:5]([N+:19]([O-:21])=[O:20])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 60993N,N-DiethylethylenediamineHCID 13590117HCID 13590117, compound

Product 1

HCID 13590120HCID 13590120, compound

Procedure

1-[[2-(Dimethylamino)ethyl]amino]-6-methoxy-4-nitro-9H-thioxanthen-9-one was prepared similarly from 0.99 g of 1-chloro-6-methoxy-4-nitrothioxanthone and 0.67 g of N,N-diethylethylenediamine affording 0.98 g, mp 144°-145°.

Sources & evidence

ORD record
ord-05fd480ba4f145cbba503a3eea225f0d
Source dataset
uspto-grants-1986_04
Patent number
US04582851

Reaction notes

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