N,N-Diethylethylenediamine → HCID 23325523, compound

HRID 1380618Notes

Reaction equation

HRID 1380618 reaction equation
Cl[C:2]1[C:15]2[C:14](=[O:16])[C:13]3[C:8](=[CH:9][CH:10]=[C:11]([OH:17])[CH:12]=3)[S:7][C:6]=2[C:5]([N+:18]([O-:20])=[O:19])=[CH:4][CH:3]=1.[CH2:21]([N:23]([CH2:27][CH3:28])[CH2:24][CH2:25][NH2:26])[CH3:22]>>[CH2:21]([N:23]([CH2:27][CH3:28])[CH2:24][CH2:25][NH:26][C:2]1[C:15]2[C:14](=[O:16])[C:13]3[C:8](=[CH:9][CH:10]=[C:11]([OH:17])[CH:12]=3)[S:7][C:6]=2[C:5]([N+:18]([O-:20])=[O:19])=[CH:4][CH:3]=1)[CH3:22]

Participants

3

Reactant 2

HCID 60993N,N-DiethylethylenediamineHCID 135901181-Chloro-7-hydroxy-4-nitro-9H-thioxanthen-9-one

Product 1

HCID 23325523HCID 23325523, compound

Procedure

1-[[2-(Diethylamino)ethyl]amino]-7-hydroxy-4-nitro-9H-thioxanthen-9-one was prepared similarly from 10 g of 1-chloro-7-hydroxy-4-nitrothioxanthone and 8.3 g of N,N-diethylethylenediamine to provide 7.3 g as a tan solid which was used without further purification.

Workup

  1. customto provide 7.3 g as a tan solid which
  2. customwas used without further purification

Sources & evidence

ORD record
ord-0c26ba066c464592a85d547630f2ac91
Source dataset
uspto-grants-1986_04
Patent number
US04582851

Reaction notes

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