Sodium Hydroxide → HCID 5216267, compound

HRID 1380626Notes

Reaction equation

HRID 1380626 reaction equation
Cl.[NH2:2][C:3]1[S:4][CH2:5][CH:6]([CH2:8][C:9]([OH:11])=[O:10])[N:7]=1.[OH-].[Na+]>O>[NH2:2][C:3]1[S:4][CH2:5][CH:6]([CH2:8][C:9]([OH:11])=[O:10])[N:7]=1

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 13590072HCID 13590072, compound

Product 1

HCID 5216267HCID 5216267, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
5 °C

Procedure

A solution of 1.965 g. (0.010 mole) 2-(2-amino-2-thiazolin-4-yl)acetic acid hydrochloride in 150 ml. water is titurated with an equimolar amount of 1.0N sodium hydroxide solution. The resulting mixture is stirred with cooling at 5° C. for two hours then filtered. The sodium salt is washed with cold water, ethanol and dried.

Workup

  1. filtrationthen filtered
  2. washThe sodium salt is washed with cold water, ethanol
  3. customdried

Sources & evidence

ORD record
ord-fed1069298a64e9eb8b12fc59a7d90dc
Source dataset
uspto-grants-1986_04
Patent number
US04582907

Reaction notes

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