HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-Methylisatin → HCID 13519800, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-Methylisatin | HCID 14313 | — |
| Reactant | Bromine | HCID 24408 | — |
| Solvent | 1,1-Dichloroethane | HCID 6365 | — |
| Product | HCID 13519800 | HCID 13519800 | — |
Reaction Steps
The 7-methylisatin (16.1 g, 0.1 mole) is suspended in dichloroethane (2000 ml) and the suspension is heated and irradiated with a high intensity light source to the reflux point. Bromine (24.3 g, 0.15 mole) is added dropwise over a one hour period.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04582909 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-3d1226a631f44ba7b1d6919d1d0d9c0d |
| Source note | uspto-grants-1986_04 |