HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 2,4,8,10-Tetra-t-butyl-6,12-dimethyl-12H-dibenzo[d,g][1,3,2]dioxasilocin
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2,2'-Ethylidenebis(4,6-di-tert-butylphenol) | HCID 118899 | — |
| Reactant | (Dichloromethyl)silane | HCID 57353436 | — |
| Product | 2,4,8,10-Tetra-t-butyl-6,12-dimethyl-12H-dibenzo[d,g][1,3,2]dioxasilocin | HCID 102330270 | — |
Reaction Steps
Utilizing the procedure of Example 1, this compound is prepared from 23.0 grams (0.20 mole) dichloromethylsilane, 87.7 grams (0.20 mole) 2,2'-ethylidene-bis(4,6-di-t-butylphenol) and 40.5 grams (0.40 mole) of triethylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04582870 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-bbf857b01b444d4ea6f3d395a0e475ee |
| Source note | uspto-grants-1986_04 |