Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chlorine → 1-Chloro-4-(trifluoromethoxy)benzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chlorine | HCID 24526 | — |
| 반응물 | 1-Nitro-4-(trifluoromethoxy)benzene | HCID 522405 | — |
| 생성물 | 1-Chloro-4-(trifluoromethoxy)benzene | HCID 2777273 | 83% |
반응 단계
Chlorine and p-nitrotrifluoromethoxybenzene (10.7 parts) were fed simultaneously at a molar ratio of 3:1, Cl2 :organic reactant, into a vapor phase reactor maintained at 300° to 320° C. over a 30 minute period to yield 8.2 parts of p-chlorotrifluoromethoxybenzene (83% yield). The structure of the product was confirmed by gas chromatographic-mass spectrum and F19 nuclear magnetic resonance analysis.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04582948 |
| 출처 데이터셋 | uspto-grants-1986_04 |
| ORD ID | ord-4b28e585bc67489cb3e1fb911d51625c |
| 출처 메모 | uspto-grants-1986_04 |