HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → HCID 13284513, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 136332139 | HCID 136332139 | — |
| Product | HCID 13284513 | HCID 13284513 | — |
Reaction Steps
Prepared analogously to Example 56 from 2-(2'-dimethylamino-4'-hydroxy-phenyl)-imidazo[4,5-b]pyridine dihydrochloride and methanesulfonyl chloride. The product was purified over silica gel column [eluant: first methylene chloride, then methylene chloride/ethanol (50:1)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04582837 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-6102e168a81345f6a94c95bb09ed3ab9 |
| Source note | uspto-grants-1986_04 |