Acetone → Allylamine hydrochloride

HRID 1380792Notes

Reaction equation

HRID 1380792 reaction equation
[ClH:1].[N:2]([CH2:10][CH:11]([C:13](=[NH:15])N)[CH3:12])=NCC(C(=N)N)C.[CH3:16][C:17]([CH3:19])=O>>[ClH:1].[CH2:10]([NH2:2])[CH:11]=[CH2:12].[ClH:1].[CH2:19]([NH:15][CH2:13][CH:11]=[CH2:12])[CH:17]=[CH2:16]

Participants

4

Reactant 2

HCID 180AcetoneHCID 22051839HCID 22051839, compound

Product 2

HCID 82291Allylamine hydrochlorideHCID 521977Diallylamine hydrochloride

Conditions

Temperature
60 °C

Procedure

The monomers prepared above were mixed together at a molar ratio shown in Table 1. After heating the monomer mixture to 60° C., 2.5% by weight (based on the monomer mixture) of azobis(2-amidinopropane) hydrochloride was added, and polymerization was carried out for 24 hours. After the reaction, the solution was added into acetone to form a precipitate, and the precipitate was collected by filtration with a glass filter and dried under reduced pressure. Thus, a copolymer of monoallylamine hydrochloride and diallylamine hydrochloride was obtained.

Workup

  1. customThe monomers prepared
  2. additionabove were mixed together at a molar ratio
  3. additionwas added
  4. custompolymerization
  5. customAfter the reaction
  6. customto form a precipitate
  7. filtrationthe precipitate was collected by filtration with a glass
  8. filtrationfilter
  9. customdried under reduced pressure

Sources & evidence

ORD record
ord-5ec663a9bdcf4b5ab7a60f789ee1ccc2
Source dataset
uspto-grants-1986_04
Patent number
US04583989

Reaction notes

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