HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-chloroacetoacetate → HCID 178494252, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-chloroacetoacetate | HCID 36240 | — |
| Reactant | Carbamimidic acid, methyl ester, hydrochloride (1:1) | HCID 3083899 | — |
| Product | HCID 178494252 | HCID 178494252 | — |
Reaction Steps
Analogously to the process described in Example 113, O-methylisourea hydrochloride or hydrosulphate is reacted with methyl 4-chloroacetoacetate in order to produce 4-chloromethyl-6-hydroxy-2-methoxy-pyrimidine, m.p. 154°-155° C., which is required as the starting material in Examples 68, 69 and 77.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04584295 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-a4028b126a79412ba20df64ffc2d5794 |
| Source note | uspto-grants-1986_04 |