Ethanol → 1-Amino-3-[N-methyl-N-(6,7-dimethoxy-1,2,3,4-tetrahydronaphth-2-yl)-amino]-propane

HRID 1380869Notes

Reaction equation

HRID 1380869 reaction equation
CO[C:3]1[C:12]([O:13][CH3:14])=[CH:11][CH:10]=[C:9]2[C:4]=1[CH2:5][CH2:6][CH:7]([NH:15][CH3:16])[CH2:8]2.[CH2:17]([OH:19])C>>[NH2:15][CH2:7][CH2:6][CH2:5][N:15]([CH3:16])[CH:7]1[CH2:6][CH2:5][C:4]2[C:9](=[CH:10][C:11]([O:19][CH3:17])=[C:12]([O:13][CH3:14])[CH:3]=2)[CH2:8]1

Participants

3

Reactant 2

HCID 702EthanolHCID 306585,6-Dimethoxy-N-methyl-1,2,3,4-tetrahydronaphthalen-2-amine

Product 1

HCID 150452791-Amino-3-[N-methyl-N-(6,7-dimethoxy-1,2,3,4-tetrahydronaphth-2-yl)-amino]-propane

Procedure

Rf value: 0.27 (alumina, eluant: 95 parts by volume of methylene chloride+5 parts by volume of ethanol).

Sources & evidence

ORD record
ord-e52bd13173354fc88869021bc8cd767e
Source dataset
uspto-grants-1986_04
Patent number
US04584293

Reaction notes

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