HCID 12381618, compound → HCID 13579649, compound

HRID 1380881Notes

Reaction equation

HRID 1380881 reaction equation
[CH3:1][NH:2][CH:3]1[CH2:12][CH2:11][C:10]2[C:5](=[CH:6][C:7]([O:15][CH3:16])=[C:8]([O:13][CH3:14])[CH:9]=2)[CH2:4]1.[CH3:17][O:18][C:19]1[C:34]([O:35][CH3:36])=[CH:33][C:22]2[CH2:23][C:24](=[O:32])[N:25]([CH2:28][CH2:29][CH2:30]Cl)[CH2:26][CH2:27][C:21]=2[CH:20]=1>>[CH3:17][O:18][C:19]1[C:34]([O:35][CH3:36])=[CH:33][C:22]2[CH2:23][C:24](=[O:32])[N:25]([CH2:28][CH2:29][CH2:30][N:2]([CH3:1])[CH:3]3[CH2:12][CH2:11][C:10]4[C:5](=[CH:6][C:7]([O:15][CH3:16])=[C:8]([O:13][CH3:14])[CH:9]=4)[CH2:4]3)[CH2:26][CH2:27][C:21]=2[CH:20]=1

Participants

3

Reactant 2

HCID 12381618HCID 12381618, compoundHCID 130925103-(3-Chloropropyl)-7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one

Product 1

HCID 13579649HCID 13579649, compound

Procedure

The title compound is prepared analogously to Example 1 by reacting 2-methylamino-6,7-dimethoxy-1,2,3,4-tetrahydronaphthalene with 1-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-3-chloro-propane. Mp: 236°-238° C.

Sources & evidence

ORD record
ord-07c8a814790e4b0fb61d9bda7a8e61ce
Source dataset
uspto-grants-1986_04
Patent number
US04584293

Reaction notes

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