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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1380884Generated: November 2, 2026

3-(3-Chloropropyl)-7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one → HCID 23324582, compound

https://huagongshe.com/reaction/1380884

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-(3-Chloropropyl)-7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-oneHCID 13092510—
Reactant2-NAPHTHALENAMINE, 1,2,3,4-TETRAHYDRO-N-METHYL-HCID 13579644—
SolventTriethylamineHCID 8471—
ProductHCID 23324582HCID 23324582—

Reaction Steps

The title compound is prepared analogously to Example 1 by reacting 1-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-3-chloropropane, triethylamine and 2-methylamino-1,2,3,4-tetrahydronaphthalene. Mp: 140°-142° C. (decomp.).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04584293
Source datasetuspto-grants-1986_04
ORD IDord-ce35e18de70740af9705c02005ce8714
Source noteuspto-grants-1986_04