HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → N-2-Picolylidene-o-nitroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-Nitroaniline | HCID 6946 | — |
| Reactant | 2-Pyridinecarboxaldehyde | HCID 14273 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N-2-Picolylidene-o-nitroaniline | HCID 13423752 | — |
Reaction Steps
27.6 g of o-nitroaniline and 21.4 g of 2-pyridine aldehyde are heated in 200 ml of toluene for 10 hours, and the water formed is collected by means of a water separator. 500 ml of diethyl ether are then added to the solution, and the crystals which precipitate are filtered off with suction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04585775 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-17b56408cf3e4642a6715513f8e1c1ed |
| Source note | uspto-grants-1986_04 |