HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 13812Generated: October 27, 2026
Dimethylformamide dimethyl acetal → 1-(2-Chlorophenyl)-2-(4-chlorophenyl)-3-(dimethylamino)prop-2-en-1-one
https://huagongshe.com/reaction/13812
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | 1-(2-Chlorophenyl)-2-(4-chlorophenyl)ethanone | HCID 348312 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 1-(2-Chlorophenyl)-2-(4-chlorophenyl)-3-(dimethylamino)prop-2-en-1-one | HCID 68658840 | — |
Reaction Steps
To 13.2 g of 1-(2-chlorophenyl)-2-(4-chlorophenyl)ethanone in 100 mL of DMF was added 23.8 g of N,N-dimethyformamide dimethyl acetal. The mixture was stirred at 75° C. for 16 hours. The solution was then concentrated and used without further purification in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07728141B2 |
|---|
| Source dataset | uspto-grants-2010_06 |
|---|
| ORD ID | ord-34f9447a81c246bab19aae29a19b928f |
|---|
| Source note | uspto-grants-2010_06 |
|---|
