HRID1381482

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：OC[C@H]1OC2C3[C@@H](CO)OC(O[C@H]4[C@H](O)[C@@H](O)[C@@H](O[C@H]5[C@H](O)[C@@H](O)[C@@H](O[C@H]6[C@H](O)[C@@H](O)[C@@H](O[C@H]7[C@H](O)[C@@H](O)[C@@H](O[C@H]8[C@H](O)[C@@H](O)[C@@H](O[C@H]9[C@H](O)[C@@H](O)C(OC1[C@H](O)[C@H]2O)O[C@@H]9CO)O[C@@H]8CO)O[C@@H]7CO)O[C@@H]6CO)O[C@@H]5CO)O[C@@H]4CO)[C@H](O)[C@H]3O

HCID44431027

未命名化合物

PRODUCTS

生成物

$结构：CC/C=C\C/C=C\C/C=C\C/C=C\C/C=C\CCCC(=O)O$

HCID446284

Timnodonic acid

C20H30O2

AUXILIARIES

试剂、催化剂与溶剂

结构：OC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O

溶剂HCID6255

beta-Maltose

C12H22O11

2 次

PROCEDURE

实验过程

Four parts of gamma-cyclodextrin powder was dissolved in 100 parts of an aqueous maltose solution, maltose content of 96.5%, d.s.b., moisture content of 18%, and the solution was mixed with 4 parts of eicosapentaenoic triglyceride and a beta-maltose hydrate seed. The mixture was crystallized, solidified, aged, pulverized and dehydrated by the method in Example 3.

WORKUP

后处理

customThe mixture was crystallized

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-abe61f4ee30246cfbfb6d138254b60ad
来源数据集: uspto-grants-1989_02
DOI: 10.6084/m9.figshare.5104873.v1
专利: US04803077
来源说明: uspto-grants-1989_02

反应 SMILES

C(O)[C@H]1O[C@@H]2O[C@H]3[C@H](O)[C@@H](O)[C@@H](O[C@H]4[C@H](O)[C@@H](O)[C@@H](O[C@H]5[C@H](O)[C@@H](O)C(O[CH:36]6[C@H:41](O)[C@@H:40](O)[CH:39]([CH:44]7[C@H:49](O)[C@@H:48](O)[CH:47]([O:52][C@H]8[C@H](O)[C@@H](O)[C@@H](O[C@H]9[C@H](O)[C@@H](O)[C@@H](O[C@H]1[C@H](O)[C@H]2O)O[C@@H]9CO)O[C@@H]8CO)[O:46][C@@H]7CO)O[C@@H:37]6[CH2:77]O)O[C@@H]5CO)O[C@@H]4CO)O[C@@H]3CO>C(O)[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O>[CH3:77][CH2:37]/[CH:36]=[CH:41]\[CH2:40]/[CH:39]=[CH:44]\[CH2:49]/[CH:48]=[CH:47]\[CH2:77]/[CH:37]=[CH:36]\[CH2:41]/[CH:40]=[CH:39]\[CH2:44][CH2:49][CH2:48][C:47]([OH:46])=[O:52]