HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Butanol → N,N-dimethyl-N'-(2,3-dihydrobenzofuran-2-ylmethyl)-1,3-propanediamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Butanol | HCID 263 | — |
| Edukt | N,N-Dimethyl-1,3-propanediamine | HCID 7993 | — |
| Edukt | p-Toluenesulfonate | HCID 85570 | — |
| Produkt | N,N-dimethyl-N'-(2,3-dihydrobenzofuran-2-ylmethyl)-1,3-propanediamine | HCID 14099475 | — |
Reaktionsschritte
Finally, 23.5 g (0.075 mol) of the above tosylate and 38.6 g (0.378 mol) of 3-(dimethylamino)propylamine were suspended in 150 ml of butanol, and the mixture was brought to reflux until the tosylate had disappeared.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04803219 |
| Quelldatensatz | uspto-grants-1989_02 |
| ORD ID | ord-dc2673a0945143cc9b81d177e7e27f7a |
| Quellennotiz | uspto-grants-1989_02 |