HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 21276194, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 12803100 | HCID 12803100 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21276194 | HCID 21276194 | — |
Reaction Steps
A solution of 2.0 g (0.014 mole) of benzoyl chloride in THF was treated with 10 ml pyridine followed by 2.43 g (0.014 mole) of 5-aminoindole-3-acetonitrile, Example 1, and stirred 18 hr. The solvent was removed in vacuo and crude product recrystallized from EtOH to give product used directly in next step below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04803218 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-be10acb836414840bd53fe615ca1833e |
| Source note | uspto-grants-1989_02 |