Dichloromethane → HCID 21276355, compound

HRID 1381657Notes

Reaction equation

HRID 1381657 reaction equation
O[CH2:2][C:3]1[C:16]2[O:15][C:14]3[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=3)[N:8]([CH:17]([C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)[CH3:18])[C:7]=2[CH:6]=[CH:5][CH:4]=1.C(Cl)[Cl:26]>>[Cl:26][CH2:2][C:3]1[C:16]2[O:15][C:14]3[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=3)[N:8]([CH:17]([C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)[CH3:18])[C:7]=2[CH:6]=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 6344DichloromethaneHCID 21276372HCID 21276372, compound

Product 1

HCID 21276355HCID 21276355, compound

Procedure

4-hydroxymethyl-N-(α-phenylethyl)phenoxazine (Example 4) dissolved in 50 ml of dry methylene chloride. The reaction mixture was stirred at room temperature under anhydrous conditions for 1 hour and the solvent removed under vacuo, to yield a solution of

Workup

  1. customthe solvent removed under vacuo
  2. customto yield a solution of

Sources & evidence

ORD record
ord-801454d64f4d4e1cafbe6c046d8a33b7
Source dataset
uspto-grants-1989_02
Patent number
US04803269

Reaction notes

Loading…