HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-2-methyl-1,3-propanediol → 2-((4,5-Dichloro-9-anthracenylmethyl)amino)-2-methyl-1,3-propanediol hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-2-methyl-1,3-propanediol | HCID 1531 | — |
| Reactant | 4,5-Dichloro-9-anthraldehyde | HCID 600741 | — |
| Product | 2-((4,5-Dichloro-9-anthracenylmethyl)amino)-2-methyl-1,3-propanediol hydrochloride | HCID 13375301 | — |
Reaction Steps
Using the reductive amination procedure outlined in 1, 4,5-dichloro-9-anthracenecarbaldehyde and 2-methyl-2-amino-1,3-propanediol (Aldrich) gave 2-((4,5-dichloro-9-anthracenylmethyl)amino)-2-methyl-1,3-propanediol hydrochloride mp 239.5°-240.5° (dec), (EtOH/Et2O), (C, H, Cl, N).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04803226 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-bf148e56ae2545feade02f6c6a092581 |
| Source note | uspto-grants-1989_02 |