HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tris(hydroxymethyl)aminomethane → HCID 14391238, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tris(hydroxymethyl)aminomethane | HCID 6503 | — |
| Reactant | 10-Chloro-9-anthraldehyde | HCID 82703 | — |
| Solvent | Diethyl ether ethanol | HCID 21585056 | — |
| Product | HCID 14391238 | HCID 14391238 | — |
Reaction Steps
Using the reductive amination procedure described in 1, 10-chloroanthracene-9-carbaldehyde (Aldrich) and tris(hydroxymethyl)aminomethane (Aldrich) gave 2-(((10-chloro-9-anthracenyl)methyl)amino)-2-hydroxymethyl-1,3-propanediol hydrochloride, mp 251°-254° (dec), (EtOH/Et2O), (C, H, Cl, N).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04803221 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-d1cb17fb81104ffba049a1975296c3e1 |
| Source note | uspto-grants-1989_02 |