HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 10-Ethoxy-9-anthracenecarbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 10-Chloro-9-anthraldehyde | HCID 82703 | — |
| Reactant | Sodium ethoxide | HCID 2723922 | — |
| Reactant | 10-Methoxyanthracene-9-carbaldehyde | HCID 13090044 | — |
| Solvent | Methylenechloride Hexane | HCID 21226440 | — |
| Product | 10-Ethoxy-9-anthracenecarbaldehyde | HCID 13375404 | — |
Reaction Steps
Using the procedure outlined in 13A, except that NaOEt (Aldrich)/EtOH was used instead of NaOCH3 /CH3OH, 10-chloro-9-anthraldehyde (Aldrich) gave 10-ethoxy-9-anthracenecarbaldehyde mp 88°-90°, (CH2Cl2 /hexane) (C, H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04803221 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-66c0691dc572494e9c7f08227d83301d |
| Source note | uspto-grants-1989_02 |