HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-2-ethyl-1,3-propanediol → 2-Ethyl-2-((3-fluoranthenylmethyl)amino)-1,3-propanediol hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-2-ethyl-1,3-propanediol | HCID 8282 | — |
| Reactant | 3-Fluoranthenecarboxaldehyde | HCID 181113 | — |
| Reactant | 773U82 Hydrochloride | HCID 3024572 | — |
| Product | 2-Ethyl-2-((3-fluoranthenylmethyl)amino)-1,3-propanediol hydrochloride | HCID 13375363 | — |
Reaction Steps
Using the reductive amination procedure described in 1D, 3-fluoranthenecarbaldehyde (1A) and 2-amino-2-ethyl-1,3-propanediol (Aldrich) gave 2-ethyl-2-((3-fluoranthenylmethyl)amino)-1,3-propanediol hydrochloride mp 250°-252° (dec), (CH3OH/Et2O), (C, H, Cl, N).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04803222 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-03f5c27e6df442b7b66c5efe860cf4df |
| Source note | uspto-grants-1989_02 |