HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1381926Generated: November 2, 2026
Ethyl Acetate → Acetamide, N-(2-amino-2-methylpropyl)-
https://huagongshe.com/reaction/1381926
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | 2-Methylpropylenediamine | HCID 13128 | — |
| Product | Acetamide, N-(2-amino-2-methylpropyl)- | HCID 9793774 | 57.4% |
Reaction Steps
A mixture of 26.4 g (0.3 mol) of ethyl acetate and 79.2 g (0.9 mole) of 1,2-diamino-2-methylpropane was heated at 100° C. in a pressured bomb for 36 hours. The reaction mixture was evaporated in vacuo and distilled to give 22.4 g (57.4%) of product which had a boiling point of 100° C. at 0.1 mmHg. This product was identified by NMR and IR spectroscopy.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04804677 |
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| Source dataset | uspto-grants-1989_02 |
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| ORD ID | ord-1e767413ad63450f9fbdbd969bb30853 |
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| Source note | uspto-grants-1989_02 |
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