Sodium Hydroxide → HCID 178488104, compound

HRID 1381971Notes

Reaction equation

HRID 1381971 reaction equation
Cl.[CH3:2][O:3][C:4]1[C:13]([O:14][CH3:15])=[CH:12][CH:11]=[C:10]2[C:5]=1[C:6]([CH3:17])=[N:7][C:8](=[O:16])[NH:9]2.[OH-].[Na+]>O>[CH3:2][O:3][C:4]1[C:13]([O:14][CH3:15])=[CH:12][CH:11]=[C:10]2[C:5]=1[C:6]([CH3:17])=[N:7][C:8](=[O:16])[NH:9]2

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 178488105HCID 178488105, compound

Product 1

HCID 178488104HCID 178488104, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

5,6-Dimethoxy-4-methyl-2(1H)-quinazolinone hydrochloride (4.26 g) was dissolved in water (500 mL) and 30% aqueous sodium hydroxide was added to adjust the pH to 7. The precipitate was collected to give 5,6-dimethoxy-4-methyl-2(1H)-quinazolinone as a yellow crystalline solid, mp 248°-249° C.

Workup

  1. customThe precipitate was collected

Sources & evidence

ORD record
ord-f4a66953adb54c3fa01d173008e00db7
Source dataset
uspto-grants-1989_02
Patent number
US04804756

Reaction notes

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