Hydrazine → 4,5-Diamino-o-anisic acid

HRID 1381976Notes

Reaction equation

HRID 1381976 reaction equation
[CH3:1][O:2][C:3]1[CH:11]=[C:10]([NH2:12])[C:9]([N+:13]([O-])=O)=[CH:8][C:4]=1[C:5]([O-:7])=[O:6].[Na+].NN>[Ni]>[CH3:1][O:2][C:3]1[CH:11]=[C:10]([NH2:12])[C:9]([NH2:13])=[CH:8][C:4]=1[C:5]([OH:7])=[O:6]

Participants

4

Reactant 2

HCID 9321HydrazineHCID 21275767Sodium 2-methoxy-4-amino-5-nitrobenzoate

Product 1

HCID 1010174,5-Diamino-o-anisic acid

Reagents, catalysts & solvents 1

HCID 935NickelCatalyst

Procedure

reacting the sodium 2-methoxy-4-amino-5-nitrobenzoate with hydrazine in the presence of Raney nickel to form 2-methoxy-4,5-diaminobenzoic acid;

Sources & evidence

ORD record
ord-ba764b23376443a8a8e98df7d39553b0
Source dataset
uspto-grants-1989_02
Patent number
US04804765

Reaction notes

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