HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → Ethyl 2-methoxyimino-2-(2-methyl-1,3-thiazol-4-yl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Ethyl 2-hydroxyimino-2-(2-methyl-1,3-thiazol-4-yl)acetate | HCID 73178131 | — |
| Product | Ethyl 2-methoxyimino-2-(2-methyl-1,3-thiazol-4-yl)acetate | HCID 53983477 | 84.5% |
Reaction Steps
Ethyl 2-hydroxyimino-2-(2-methyl-1,3-thiazol-4-yl)acetate (anti isomer) (0.3 g.) and dimethyl sulfate (0.18 g.) were reacted according to a similar manner to that of Preparation (8-5) to give pale yellow oil of ethyl 2-methoxyimino-2-(2-methyl-1,3-thiazol-4-yl)acetate (anti isomer) (0.27 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04804752 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-fdfc7f5f27684bff8a005be7ff404494 |
| Source note | uspto-grants-1989_02 |