HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178471920, compound → 3-benzoyl-8-methoxy-4(1H)-quinolone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178471920 | HCID 178471920 | — |
| Solvent | Diphenyl Ether | HCID 7583 | — |
| Product | 3-benzoyl-8-methoxy-4(1H)-quinolone | HCID 11778353 | 93.5% |
Reaction Steps
Ethyl 2-benzoyl-3-(2-methoxyphenylamino)acrylate (6.0 g, 0.018 mol) was added in portions to boiling diphenyl ether (100 ml) and heated under reflux for 45 minutes. The reaction mixture was allowed to cool and diluted with petroleum ether to afford the crystalline 3-benzoyl-8-methoxy-4(1H)-quinolone (4.7 g, 91%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04806549 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-3ca8a8a59adb420eb4fefa3c6892f6d9 |
| Source note | uspto-grants-1989_02 |