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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1382313Generated: October 28, 2026

2-Methoxyaniline → Ethyl3-(2-methoxyphenylamino)acrylate

https://huagongshe.com/reaction/1382313

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-MethoxyanilineHCID 7000—
ReactantEthyl propiolateHCID 12182—
SolventEthanolHCID 702—
ProductEthyl3-(2-methoxyphenylamino)acrylateHCID 67899433100%

Reaction Steps

o-Anisidine (57 ml, 0.5 mol) and ethyl propiolate (51 ml, 0.5 mol) were heated together under reflux in ethanol (200 ml) for 3 hours. The solvent was evaporated to afford ethyl 3-(2-methoxyphenylamino)acrylate as a yellow oil (55 g, 100%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04806550
Source datasetuspto-grants-1989_02
ORD IDord-2f70d961b5194ba6b147d0b232c0439e
Source noteuspto-grants-1989_02