4-Methoxyphenol → HCID 13120353, compound

HRID 1382384Notes

Reaction equation

HRID 1382384 reaction equation
Cl[CH2:2][CH:3]([OH:7])[CH2:4][CH2:5][Cl:6].[CH3:8][O:9][C:10]1[CH:15]=[CH:14][C:13]([OH:16])=[CH:12][CH:11]=1>>[Cl:6][CH2:5][CH2:4][CH:3]([OH:7])[CH2:2][O:16][C:13]1[CH:14]=[CH:15][C:10]([O:9][CH3:8])=[CH:11][CH:12]=1

Participants

3

Reactant 2

HCID 90154-MethoxyphenolHCID 170211,4-Dichloro-2-butanol

Product 1

HCID 13120353HCID 13120353, compoundYield 42%

Procedure

Utilizing the procedure of Preparation 21, 1,4-dichloro-2-butanol was reacted with 4-methoxyphenol to give white title compound, m.p. 65°-68° C. in 42% yield. The recrystallizing solvent was diethyl ether.

Sources & evidence

ORD record
ord-d57d15810b9645cc86d7e235eed9edbb
Source dataset
uspto-grants-1989_02
Patent number
US04806555

Reaction notes

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