HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 14422843, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | N-(3-methoxyphenyl)piperazine | HCID 81430 | — |
| Reactant | 4-Chloro1-phenoxy-2-butanol | HCID 13120342 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 14422843 | HCID 14422843 | 46.3% |
Reaction Steps
This compound was prepared according to the procedure of Example 78. A mixture of 3.8 g (0.02 mole) of 1-(3-methoxyphenyl)piperazine, 4.0 g (0.02 mole) of 4-chloro-1-phenoxy-2-butanol and 8.0 g (0.075 mole) of anhydrous sodium carbonate in 150 ml of 1-butanol gave 3.3 g (45%) of off-white powder, m.p. 58°-60° C. Recrystallizing solvent used was diethyl ether-petroleum ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04806555 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-56702164366e4560bf0c75559070e59a |
| Source note | uspto-grants-1989_02 |