Phosphoric Acid → HCID 22841499, compound

HRID 1382491Notes

Reaction equation

HRID 1382491 reaction equation
P(=O)(O)(O)O.[Cl:6][CH:7]([Cl:23])[C:8]([NH:10][CH:11]([C@@H:13]([C@H:15]([C@@H:17]([C@@H:19]([CH2:21][OH:22])[OH:20])[OH:18])[OH:16])[OH:14])O)=[O:9]>O>[Cl:6][CH:7]([Cl:23])[C:8]([NH:10][CH2:11][C@H:13]([OH:14])[C@@H:15]([OH:16])[C@H:17]([OH:18])[C:19](=[O:20])[CH2:21][OH:22])=[O:9]

Participants

4

Reactant 2

HCID 1004Phosphoric AcidHCID 131715864HCID 131715864, compound

Product 1

HCID 22841499HCID 22841499, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

To a suspension of 40 g of Gluconobacter oxidans ssp. suboxidans (DSM 50049) in 1 l of tap water, brought to pH 4.5 with phosphoric acid, are added at 32° C. and 700 rpm with venting of 3 l of air/hour 20 g of N-dichloroacetylaminosorbitol. The reaction has ended after 10 hours, and the cells are then centrifuged off, washed twice with 100 ml of methanol each time and discarded. The methanol extracts are combined with the aqueous supernatant and concentrated to dryness in vacuo.

Workup

  1. additionare added at 32° C.
  2. washwashed twice with 100 ml of methanol each time
  3. concentrationconcentrated to dryness in vacuo

Sources & evidence

ORD record
ord-a473e86caf9549588b3c56ea51ba8e2e
Source dataset
uspto-grants-1989_02
Patent number
US04806650

Reaction notes

Loading…