Ethyl 2-oxocyclohexylacetate → HCID 15157536, compound
Reaction equation
Cl.[Cl:2][C:3]1[CH:18]=[CH:17][C:6]([CH2:7][N:8]([C:10]2[CH:15]=[CH:14][C:13]([Br:16])=[CH:12][CH:11]=2)N)=[CH:5][CH:4]=1.CC[O:21][C:22]([CH2:24][CH:25]1[C:30](=O)[CH2:29][CH2:28][CH2:27][CH2:26]1)=[O:23]>>[Br:16][C:13]1[CH:12]=[C:11]2[C:10](=[CH:15][CH:14]=1)[N:8]([CH2:7][C:6]1[CH:17]=[CH:18][C:3]([Cl:2])=[CH:4][CH:5]=1)[C:26]1[CH:25]([CH2:24][C:22]([OH:23])=[O:21])[CH2:30][CH2:29][CH2:28][C:27]2=1Participants
3
Procedure
Following the procedure of Example 1, but using 1-(4-chlorobenzyl)-1-(4-bromophenyl)hydrazine hydrochloride and ethyl 2-cyclohexanone acetate as starting materials, the title compound was prepared.
Sources & evidence
- ORD record
- ord-8b9f2801b8ac47c4861d602f6a8cdb2e
- Source dataset
- uspto-grants-1989_02
- Patent number
- US04808608
Reaction notes
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