Ethyl 2-oxocyclohexylacetate → HCID 17913378, compound
Reaction equation
Cl.[Cl:2][C:3]1[CH:19]=[CH:18][C:6]([CH2:7][N:8]([C:10]2[CH:15]=[CH:14][C:13]([S:16][CH3:17])=[CH:12][CH:11]=2)N)=[CH:5][CH:4]=1.CC[O:22][C:23]([CH2:25][CH:26]1[C:31](=O)[CH2:30][CH2:29][CH2:28][CH2:27]1)=[O:24]>>[Cl:2][C:3]1[CH:19]=[CH:18][C:6]([CH2:7][N:8]2[C:27]3[CH:26]([CH2:25][C:23]([OH:24])=[O:22])[CH2:31][CH2:30][CH2:29][C:28]=3[C:15]3[C:10]2=[CH:11][CH:12]=[C:13]([S:16][CH3:17])[CH:14]=3)=[CH:5][CH:4]=1Participants
3
Procedure
Following the procedure of Example 1, but using 1-(4-chlorobenzyl)-1-(4-methylthiophenyl)hydrazine hydrochloride and ethyl 2-cyclohexanone acetate as starting materials, the title compound was prepared.
Sources & evidence
- ORD record
- ord-2da296c0ed974e1c95d1fde69e058f9d
- Source dataset
- uspto-grants-1989_02
- Patent number
- US04808608
Reaction notes
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