1-(p-Chlorobenzyl)-1-(4-fluorophenyl)hydrazine hydrochloride → HCID 14372530, compound

HRID 1382834Notes

Reaction equation

HRID 1382834 reaction equation
Cl.[Cl:2][C:3]1[CH:18]=[CH:17][C:6]([CH2:7][N:8]([C:10]2[CH:15]=[CH:14][C:13]([F:16])=[CH:12][CH:11]=2)N)=[CH:5][CH:4]=1.[C:19]([OH:22])(=[O:21])[CH3:20].C([CH:25]1[CH2:30][CH2:29][CH:28]([CH3:31])[CH2:27][C:26]1=O)C>>[Cl:2][C:3]1[CH:18]=[CH:17][C:6]([CH2:7][N:8]2[C:25]3[CH:30]([CH2:20][C:19]([OH:22])=[O:21])[CH2:29][CH:28]([CH3:31])[CH2:27][C:26]=3[C:15]3[C:10]2=[CH:11][CH:12]=[C:13]([F:16])[CH:14]=3)=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 145912421-(p-Chlorobenzyl)-1-(4-fluorophenyl)hydrazine hydrochlorideHCID 67867503HCID 67867503, compound

Product 1

HCID 14372530HCID 14372530, compound

Procedure

Following the procedure of Example 1, but using 1-(4-chlorobenzyl)-1-(4-fluorophenyl)hydrazine hydrochloride and ethyl 4-methyl-2-cyclohexanone acetate as starting materials, the title compound was prepared. m.p. 205°-206° C.

Sources & evidence

ORD record
ord-6dac2c47f4b64e8eae10218509ee4cf2
Source dataset
uspto-grants-1989_02
Patent number
US04808608

Reaction notes

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