Ethyl 2-oxocyclohexylacetate → HCID 14372507, compound

HRID 1382837Notes

Reaction equation

HRID 1382837 reaction equation
[ClH:1].[CH3:2][O:3][C:4]1[CH:9]=[CH:8][C:7]([NH:10]N)=[C:6]([CH3:12])[CH:5]=1.CC[O:15][C:16]([CH2:18][CH:19]1[C:24](=O)[CH2:23][CH2:22][CH2:21][CH2:20]1)=[O:17]>>[Cl:1][C:9]1[CH:8]=[CH:7][C:6]([CH2:12][N:10]2[C:20]3[CH:19]([CH2:18][C:16]([OH:15])=[O:17])[CH2:24][CH2:23][CH2:22][C:21]=3[C:8]3[C:7]2=[C:6]([CH3:12])[CH:5]=[C:4]([O:3][CH3:2])[CH:9]=3)=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 91229Ethyl 2-oxocyclohexylacetateHCID 219977414-Methoxy-2-methylphenylhydrazine hydrochloride

Product 1

HCID 14372507HCID 14372507, compound

Procedure

Following the procedure of Example 34, but using 1-(4-methoxy-2-methylphenyl)hydrazine hydrochloride and ethyl 2-cyclohexanone acetate as starting materials, the title compound was prepared. m.p. 188°-188.5° C.

Sources & evidence

ORD record
ord-3ba7e68e9b9a476eab430a7ea99d7434
Source dataset
uspto-grants-1989_02
Patent number
US04808608

Reaction notes

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