HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Di-tert-butylphenol → HCID 14368273, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Di-tert-butylphenol | HCID 31405 | — |
| Reactant | 2-Chloro-6-methylpyridine-3-carbonyl chloride | HCID 21273637 | — |
| Product | HCID 14368273 | HCID 14368273 | 82.8% |
Reaction Steps
The similar procedure in reference example 1 by using 19 g of 2-chloro-6-methylnicotinoyl chloride, 24.7 g of 2,6-di-tertiary butylphenol and 31.3 g of anhydrous stannic chloride is performed and the obtained crude product is recrystallized from hexane to give 29.8 g of 4-(2-chloro-6-methylnicotinoyl)-2,6-di-tertiary butylphenol as pale yellow crystals, melting at 116°-117° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04808620 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-b691d903ac664fc1a32bb03a1ae7cc7b |
| Source note | uspto-grants-1989_02 |