1-Iodooctane → 3-(3,5-Di-tertiary butyl-4-hydroxyphenyl)-1-octyl-1H-pyrazolo[3,4-b]pyridine

HRID 1382886Notes

Reaction equation

[C:1]([C:5]1[CH:6]=[C:7]([C:16]2[C:24]3[C:19](=[N:20][CH:21]=[CH:22][CH:23]=3)[NH:18][N:17]=2)[CH:8]=[C:9]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:10]=1[OH:11])([CH3:4])([CH3:3])[CH3:2].[CH2:25](I)[CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32]>>[C:1]([C:5]1[CH:6]=[C:7]([C:16]2[C:24]3[C:19](=[N:20][CH:21]=[CH:22][CH:23]=3)[N:18]([CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[N:17]=2)[CH:8]=[C:9]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:10]=1[OH:11])([CH3:2])([CH3:3])[CH3:4]

Participants

Reactant 2

HCID 123801-Iodooctane

HCID 178440702HCID 178440702, compound

Product 1

HCID 1359930073-(3,5-Di-tertiary butyl-4-hydroxyphenyl)-1-octyl-1H-pyrazolo[3,4-b]pyridine

Procedure

3-(3,5-Di-tertiary butyl-4-hydroxyphenyl)-1-octyl-1H-pyrazolo[3,4-b]pyridine is prepared by reacting the compound of Example 1 with octyl iodide as yellowish brown oil in a similar manner as Example 9.

Sources & evidence

ORD record: ord-ae743d6c76a74e5d828fa9ccf9094b1b
Source dataset: uspto-grants-1989_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04808620

Reaction notes

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