HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 13983022, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 4,4,6-Trimethyl-3,4-dihydro-2H-1-benzopyran | HCID 13758110 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 13983022 | HCID 13983022 | — |
Reaction Steps
A mixture of 5.0 g (28.4 mmole) of 4,4,6-trimethylchroman, 5.55 g of purified N-bromosuccinimide and 200 ml of carbon tetrachloride was heated under reflux for 12 hours. The succinimide was removed by filtration and the solvent was removed by evaporation in vacuo to give the title compound as a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04808597 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-24ca10bc2888467ab20b995441399992 |
| Source note | uspto-grants-1989_02 |