HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21273330, compound → HCID 14372147, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21273330 | HCID 21273330 | — |
| Reactant | 3-(Furan-2-yl)-2-methylprop-2-enoic acid | HCID 53806806 | — |
| Reactant | HCID 54212216 | HCID 54212216 | — |
| Product | HCID 14372147 | HCID 14372147 | — |
Reaction Steps
The title compound was prepared according to the procedure described for 2-sulfamoyl-6-methylfuro[3.2-c]pyridin-4-(5H)-one (Example 12 Step A) except 3-(2-furanyl)-3-methylacrylic acid was substituted for 3-(2-furanyl)methacrylic acid. Title compound was obtained in 41% yield, m.p. 239°-241° C., after crystallization from methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04808595 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-883d592244404fceadbf46d0f3f1ab4a |
| Source note | uspto-grants-1989_02 |