4-chloro-6-methylfuro[3,2-c]pyridine → HCID 14372149, compound

HRID 1383001Notes

Reaction equation

HRID 1383001 reaction equation
CC1N=CC2C=COC=2C=1.Cl[C:12]1[C:17]2[CH:18]=[CH:19][O:20][C:16]=2[C:15]([CH3:21])=[CH:14][N:13]=1.ClC1C2C=COC=2C=C(C)N=1>>[CH3:21][C:15]1[C:16]2[O:20][CH:19]=[CH:18][C:17]=2[CH:12]=[N:13][CH:14]=1

Participants

4

Reactant 3

HCID 122371844-chloro-6-methylfuro[3,2-c]pyridineHCID 14005231HCID 14005231, compoundHCID 14372148HCID 14372148, compound

Product 1

HCID 14372149HCID 14372149, compound

Procedure

The title compound was prepared according to the procedure described for 6-methylfuro[3,2-c]pyridine (Example 12, step C) except 4-chloro-7-methylfuro[3,2-c]pyridine was substituted for 4-chloro-6-methylfuro[3,2-c]-pyridine. Title compound was obtained pure in 81% yield after distillation under vacuum, b.p. 74° C./2.2 mm Hg. This material crystallized, m.p. 41°-43° C.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-18cc840925b74240b954a26c050b74fc
Source dataset
uspto-grants-1989_02
Patent number
US04808595

Reaction notes

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