HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → N-(3-methyl-4-hydroxy-5-tert-butylphenylthiomethyl)phthalimide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Chloromethylphthalimide | HCID 87154 | — |
| Reactant | HCID 13547656 | HCID 13547656 | — |
| Product | N-(3-methyl-4-hydroxy-5-tert-butylphenylthiomethyl)phthalimide | HCID 14047795 | 46.3% |
Reaction Steps
The procedure of Example 1 was repeated using 8.46 grams of 3-methyl-4-hydroxy-5-tert-butylbenzenethiol, 1.72 grams of potassium hydroxide, and 8.43 grams of N-(chloromethyl)phthalimide. Recrystallization from ethyl acetate-heptane afforded 7.1 grams of product with m.p. 114°-116° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04808644 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-dee18dd548ae459485c9c510fed762b8 |
| Source note | uspto-grants-1989_02 |