HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Dimethylamino)Benzaldehyde → HCID 70351680, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Dimethylamino)Benzaldehyde | HCID 7479 | — |
| Reactant | HCID 17802483 | HCID 17802483 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 70351680 | HCID 70351680 | — |
Reaction Steps
1.49 g of 4-dimethylamino-benzaldehyde are added to a solution of 0.88 g of 1,3-diamino-2-isopropyl-imidazolium chloride in 15 ml of glacial acetic acid. After allowing the reaction mixture to stand at room temperature for 2 days, the product is crystallized out by the addition of ether and then recrystallized from ethanol. There is obtained 1,3-bis[[p-(dimethylamino)benzylidene]amino]-2-isopropyl-imidazolium chloride of melting point 241°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04808727 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-eff4aa9df71744aeba34a2cfc82575b7 |
| Source note | uspto-grants-1989_02 |