HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(Chloromethyl)-1,2,3-trimethoxybenzene → HCID 178437581, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(Chloromethyl)-1,2,3-trimethoxybenzene | HCID 77448 | — |
| Reactant | 1-Benzylideneamino-2-ethylimidazole | HCID 54091172 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178437581 | HCID 178437581 | — |
Reaction Steps
(ii.a) 2.16 g of 3,4,5-trimethoxybenzyl chloride are added to a solution of 1.99 g of 1-benzylideneamino-2-ethylimidazole in 10 ml of acetonitrile and the mixture is heated under reflux for 28 hours. The crystallized-out product is filtered and washed with ether. There is obtained 1-benzylideneamino-2-ethyl-3-(3,4,5-trimethoxybenzyl)imidazolium chloride of melting point 205°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04808727 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-1c7f6f6383944d4897226a1d3b228a87 |
| Source note | uspto-grants-1989_02 |