HuagongsheHuagongshe Chemistry Print Report · For research reference only
(+-)(2R*,3S*)-2-Methyl-2-nitro-1,3-butanediol → (+-)(2R*,3S*)-2-amino-2-methyl-1,3-butanediol acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (+-)(2R*,3S*)-2-Methyl-2-nitro-1,3-butanediol | HCID 13375424 | — |
| Reactant | (+-)(2R*,3R*)-2-amino-2-methyl-1,3-butanediol acetate | HCID 86741969 | — |
| Product | (+-)(2R*,3S*)-2-amino-2-methyl-1,3-butanediol acetate | HCID 86741966 | 93% |
Reaction Steps
Using the procedure described for 5E (+-)(2R*,3S*)-2-methyl-2-nitro-1,3-butanediol (5A) gave (+-)(2R*,3S*)-2-amino-2-methyl-1,3-butanediol acetate (93%) mp 163°-165° (C,H,N).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04808632 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-1962d4b2b9ca445ba0489b8daf21147e |
| Source note | uspto-grants-1989_02 |