HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2S)-2-hydroxy-2-(3-phenoxyphenyl)acetonitrile → HCID 86739824, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2S)-2-hydroxy-2-(3-phenoxyphenyl)acetonitrile | HCID 9837437 | — |
| Reactant | HCID 86739825 | HCID 86739825 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 86739824 | HCID 86739824 | — |
Reaction Steps
Using the procedure of Example 1, the product of Step A and (S)α-cyano-3-phenoxy-benzyl alcohol were reacted to obtain (S)α-cyano-3-phenoxy-benzyl (1R,cis) 2,2-dimethyl-3(E)-[2-bromo-3-oxo-3-ethoxy-propenyl)-cyclopropane-carboxylate with a specific rotation of [α]D20 =-70.5°±2° (c=0.7% in chloroform).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04808749 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-f35df3d30b0b4b5f9f378ce6f45814f0 |
| Source note | uspto-grants-1989_02 |