HRID1383238

反应详情

EQUATION

反应方程式

HRID 1383238 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

This compound was prepared in a manner analogous to that of Example 4, Step E, by hydrogenation of 1.0 gram (0.0027 mole) of 1-(4-chlorophenyl)-1-cyclopropyl-4-(3-phenoxyphenyl)-1-butene in the presence of 0.35 gram of Raney nickel in 75 mL of ethanol. This procedure yielded 0.8 gram of 1-(4-chlorophenyl)-1-cyclopropyl-4(3-phenoxyphenyl)butane as an a oil. The nmr spectrum was consistent with the proposed structure.

WORKUP

后处理

  1. customThis compound was prepared in a manner analogous to that of Example 4, Step E